• Українська
  • English
  • Русский
ISSN 2415-3400 (Online)
ISSN 1028-821X (Print)

A laboratory magnetometer for express measurements of magnetic hysteresis loops

Sova, KY, Vakula, AS, Polevoy, SY, Tarapov, SI
Organization: 

O.Ya. Usikov Institute for Radiophysics and Electronics of NAS of Ukraine
12 Acad. Proskury St., Kharkiv, 61085, Ukraine

V.N. Karazin Kharkiv National University
4 Svobody sq., Kharkiv, 61022, Ukraine

E-mail: katerinesova@gmail.com

https://doi.org/10.15407/rej2021.02.032
Language: english
Abstract: 

 

 

Subject and Purpose. The development of technologies for synthesis of nanoscale magnetic materials requires new techniques for measuring magnetic properties of nanoscale magnetic materials in such a way as to provide express post-synthesis measurements of magnetic properties and exclude, in doing so, any mechanical displacements of measured specimens. Despite the fact that numerous techniques exist for studying magnetic properties of materials, the development of such magnetic nanomaterials as magnetic nanoparticles faces the need in novel measuring approaches based on standard procedures. Novel express techniques are called to gain information about how magnetic properties of magnetic materials vary over time and respond to such factors as temperature, storage conditions, stabilizing agents, exposure to an external magnetic field.

Method and Methodology. In this work, magnetic hysteresis loops are registered using a newly developed technique based on the method of small disturbances (by an external magnetic field) and combining standard constructions of hysterometers and vibrating-sample magnetometers.

Results. Magnetic hysteresis loops of a bulky ferrite (brand 1SCh4) sample and a 40 μm thick YIG film have been registered using the presented technique and compared with the results obtained by the well-known technique for measuring magnetic hysteresis loops. They are in good agreement with a margin error as low as 10%, which can be further improved by means of more precise equipment. With the presented technique, the magnetization and the coercive force of Fe0.5Co0.5Fe2O4 nanoparticles not examined yet have been determined.

Conclusion. The developed technique makes it possible to study magnetic materials of various compositions including nanoscale magnets.

Keywords: magnetic hysteresis loop, magnetization, magnetometer

Manuscript submitted 21.12.2020
Radiofiz. elektron. 2021, 26(2): 32-36
Full text (PDF)

References: 
1. Soohoo, R.F., 1965. Magnetic thin films. New York, Evanston and London: Harper & Row Publishers, 316 p.
 
2. Chechernikov, V.I., 1969. Magnetic measurements. 2nd ed. Ye.I. Kondorskii ed. Moscow University publishing center, 388 p. (in Russian).
 
3. Maksimochkin, I., Trukhin, V.I., Garifullin, N.M., Khasanov, N.A., 2003. An Automated High-Sensitivity Vibrating-Coil Magnetometer. Instrum. Exp. Tech., 46(5), pp. 702-707. DOI: https://doi.org/10.1023/A:1026062310118
 
4. Shin, K.H., Park, K.I., Kim, Y., Sa-Gong, G., 2004. Vibrating sample magnetometer using a multilayer piezoelectric actuator. Phys. Status Solidi B, 241(7), pp. 1633-1636. DOI: https://doi.org/10.1002/pssb.200304666
 
5. Timofeev, V.P., Khvostov, S.S., Tsoi, G.M., Shny, V.I., 1992. UHF SQUID-magnetometer at 77 K. Cryogenics, 32, suppl. 1, pp. 517-520. DOI: https://doi.org/10.1016/0011-2275(92)90219-Z
 
6. He, D.F., Yoshizawa, M., 2003. Mobile high-Tc DC SQUID magnetometer. Physica B, 329-333, Pt. 2, pp. 1489-1490. DOI: https://doi.org/10.1016/S0921-4526(02)02403-1
 
7. Lopez-Dominguez, V., Quesada, A., Guzmán-Mínguez, J.C., Moreno, L., Lere, M., Spottorno, J., Giacomone, F., Fernández, J.F., Hernando, A., García, M.A., 2018. A simple vibrating sample magnetometer for macroscopic samples. Rev. Sci. Instrum., 89(3), pp. 034707-034713. DOI: https://doi.org/10.1063/1.5017708
 
8. Poole, C., 1997. Electron Spin Resonance: A comprehensive treatise on experimental techniques. New York: Dover Publ. ISBN-13:978-0486694443.
 
9. Gurevich, A.G., Melkov, G.A., 1996. Magnetization Oscillations and Waves. CRC Press, Boca Raton, N.Y., L., Tokyo, 445 p.
 
10. Gurevich, A.G., 1960. Ferrites at ultra-high frequencies. Moscow: Fizmatgiz Publ. (in Russian).
 
11. Chernovtsev, S.V., Belozorov, D.P., Tarapov, S.I., 2007. Magnetically controllable 1D magnetophotonic crystal in millimetre wavelength band. J. Phys. D: Appl. Phys., 40(2), pp. 295-299. DOI: https://doi.org/10.1088/0022-3727/40/2/001
 
12. Yelenich, O.V., Solopan, S.O., Trachevskii, V.V., Belous, A.G., 2013. Synthesis and Properties of AFe2O4 (A=Fe, Co, Ni, Zn) Nanoparticles Produced by Deposition from Diethylene Glycol Solution. Russ. J. Inorg. Chem., 58(8), pp. 901-905. DOI: https://doi.org/10.1134/S0036023613080068
 
13. Vakula, A.S., Kravchuk, O.A., Tarapov, S.I., Belous, A.G., 2020. Ferromagnetic resonance in Fe1-xCoxFe2O4 nanoparticles precipitated from diethyleneglycol. Radiofiz. Electron., 25(3), pp. 54-59. DOI: https://doi.org/10.15407/rej2020.03.054